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CN102048857A – Method for extracting alkaloid from Kratom
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- Summary of article content: Articles about CN102048857A – Method for extracting alkaloid from Kratom
– Google Patents The invention discloses a method for extracting alkalo from Kratom, which comprises the following steps of: 1) smashing Kratom leaves, extracting with 90 … … - Most searched keywords: Whether you are looking for CN102048857A – Method for extracting alkaloid from Kratom
– Google Patents The invention discloses a method for extracting alkalo from Kratom, which comprises the following steps of: 1) smashing Kratom leaves, extracting with 90 …
The invention discloses a method for extracting alkaloid from Kratom, which comprises the following steps of: 1) smashing Kratom leaves, extracting with 90 to 95 percent ethanol at normal temperature, combining extracts, and concentrating to obtain concentrate; 2) adding ethanol into the concentrate until the ethanol concentration is 90 (mass) percent, standing for 1 to 3 hours, centrifuging, collecting supernate, concentrating until alcohol is removed completely, and obtaining concentrated supernate; and 3) extracting the concentrated supernate with ethyl acetate for 1 to 3 times, re-extracting with chloroform for 1 to 2 times, concentrating the chloroform extract, removing the chloroform, freezing and drying to obtain Kratom alkaloid extract. The method is simple and easy to control, the total mass of the alkaloid in the obtained extract is more than 70 percent (assayed by High performance liquid chromatography (HPLC)), and the yield is 0.6 to 0.8 percent. - Table of Contents:
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how to make kratom resin
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Kratom resin/extraction tek – PsychonautWiki
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- Summary of article content: Articles about Kratom resin/extraction tek – PsychonautWiki The alkalos in kratom (the goodies you are extracting) are broken down at around 105 degrees Celsius, so your kratom mixture should never … …
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This will take a while in the kitchen/on the hob so one should be thoughtful to others who require the cooker for food prep, etc.
Never leave a stove/cooker on without being there to check it.
Finally, this tek uses only food safe materials so the extract is edible safe. - Table of Contents:
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Full Spectrum 25% Kratom Extract | Kats Botanicals
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CN102048857A – Method for extracting alkaloid from Kratom – Google Patents
From Kratom, extract alkaloidal method
Technical field The present invention relates to extraction method of active ingredients in the plant, be specifically related to from Kratom, extract alkaloidal method.
Background technology Kratom (Mitragyna specilsa) is a kind of trees in the Rubiaceae medicated cap spar platymiscium, originates in Southeast Asia (Thailand, Malaysia and Burma).From the ancient times, the people of Southeast Asian countries just with the leaves of Kratom as the medical herbs drug use.It is used as analeptic (low dosage), tranquilizer (high dose can make the people hallucinate), recreational medicine, analgesic, and the diarrhoea medicine uses, and also can be used for treating the Opium addiction. The alkaloid of the active component of Kratom for wherein containing.Go out to surpass 25 alkaloids from kratom isolation identification at present, wherein the abundantest alkaloid of content comprises three kinds of indole (indoles) and two kinds of indolones (oxindoles), these three kinds of indole are respectively mitragynine (mitragynine), speciogynine (paynanthine) and speciogynine; Two kinds of indolones are mitraphylline (mitraphylline) and speciofoline (speciofoline).Mitragynine (mitragynine) most importantly wherein, it plays pain relieving, calmness, happiness, and stimulation is arranged.The similar of mitragynine (mitragynine) is in Yohimbine, but do not have identical effect.Other biological alkali at present comprises other indole, as Ah agate’s alkali, and corynantheidine (corynanthedine), mitraversine (mitraversine), Ramulus Uncariae cum Uncis alkali (rhychophylline) and stipulatine etc. The Kratom leaves generally is to chew or made tea by warm water to drink.Also the Kratom leaves can be gone up resin isolation after by flooding and obtain the Kratom crude extract, but not see also that at present useful ethanol extracts alkaloidal relevant report from the Kratom leaves.
Summary of the invention The technical problem to be solved in the present invention provides a kind of alkaloidal method of extracting from Kratom.This method adopts ethanol to extract, and method is simple, easily control, extract obtained in alkaloidal total content can reach more than 70%. Of the present inventionly from Kratom, extract alkaloidal method, may further comprise the steps: 1) getting the Kratom leaves, pulverize, is that 90～95% alcohol at normal temperature extracts with volumetric concentration, and merge extractive liquid, concentrates, must concentrated solution; 2) add ethanol in concentrated solution, making concentration of alcohol wherein is 90% (quality), places 1～3 hour, centrifugal, collects supernatant, and being concentrated into does not have the alcohol flavor, gets concentrated supernatant; 3) the gained concentrated supernatant is used ethyl acetate extraction 1～3 time earlier, reuse chloroform extraction 1～2 time, and gained chloroform extraction liquid concentrates, and removes chloroform, and lyophilization promptly obtains the Kratom alkaloid extract. Extract in the product (being alkaloid extract) that obtains among the application, comprise the various alkaloids that contained among the plant Kratom. In the said method step 1), the number of times of extraction is 1～3 time, and solid-liquid ratio is 1: 7～10 (W/V), extracts 20～24 hours at every turn.Wherein said extracting solution is concentrated into 0.5～0.8 times of raw material weight. In the step 3), the consumption of ethyl acetate is 2～3 times of raw material weight, and the consumption of chloroform is 3～4 times of raw material weight.If the gained concentrated supernatant is thickness too, can add water earlier and necessarily dilute back reuse ethyl acetate extraction, generally concentrated supernatant is diluted with water to 0.5～0.7 times of raw material weight.The acetic acid ethyl acetate extract that obtains after being concentrated into no ethyl acetate, the reuse chloroform extraction.Similarly, if the extract of removing ethyl acetate thickness too can add water earlier and necessarily dilute back reuse chloroform extraction, the extract that generally will remove ethyl acetate is diluted with water to 0.3～0.5 times of raw material weight. Compared with prior art, the invention provides a kind of alkaloidal method of from Kratom, extracting.This method is utilized alkaloidal pure dissolubility matter among the Kratom, adopt 90～95% ethanol to extract, can make alkaloid stripping as much as possible wherein, successively use ethyl acetate and chloroform extraction behind the extracting solution precipitate with ethanol again, method is simple, easily control, alkaloidal total content can reach more than 70% (the HPLC mensuration) in the extract that obtains, and yield is 0.6～0.8% (promptly 100 gram raw materials can extract the alkaloid that obtains 0.6～0.8 gram).
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Kratom resin/extraction tek
Disclaimer: This guide is provided for informational and educational purposes only. We do not encourage you to break the law and cannot claim any responsibility for your actions.
Materials
100 grams of powdered kratom leaf (strain or blend of choosing). If dried whole leaf, then blend.
3 litres of water (tap will suffice)
Kettle (not essential, but helps)
1-2 lemons/limes (for juice)
Two medium wide-base pans
Muslin/cheese cloth (a t-shirt will work, but is not the best option)
Vinegar (the higher acid content the better) ~5% will do.
Wide-base pyrex (or ovenproof) dish
Cooking parchment is helpful.
Scraping tool (a knife, etc.)
Freezer proof tupperware/pot
Freezer
Pre-method notes
The alkaloids in kratom (the goodies you are extracting) are broken down at around 105 degrees Celsius, so your kratom mixture should never reach these temperatures. This will take a while in the kitchen/on the hob so one should be thoughtful to others who require the cooker for food prep, etc. Never leave a stove/cooker on without being there to check it. Finally, this tek uses only food safe materials so the extract is edible safe.
N.B. This method can be repeated on the washed kratom powder (the remains NOT filtered from the liquid in the final steps). However, despite the yield being reduced if already washed there it is recommended to attempt to re-wash it.
Method
Add kratom powder to just enough water to cover it. The mixture should be a thick liquid/mud with not too much water. One should mix this well. Add the juice of half a lime/lemon and/or a few dashes of vinegar and leave overnight. Add this mixture to a freezer in the freezer proof tub until frozen solid. Remove frozen kratom and add to pan. Add 1 litre boiling water. Add juice of half lemon/lime. Simmer for 1 – 2 hours, evaporating some water (about a quarter). Wait to cool and strain; keep both the water and the wet powder that didn’t pass the filter. Add the strained water to your second pan and keep simmering. Evaporate more water off. Add the kratom powder you collected when straining into the first pan. Add 1 litre boiling water and the juice from the second half of the lime/lemon. Simmer until half the water is gone. Add several dashes of vinegar to the pan with the water + powder (remember which one). Filter the water + powder for the last time (keep the kratom powder collected by the filtering for more washes or throw out). Add all the filtered water (very dark in color) to one pan and simmer until it becomes thicker than water. Pour thick alkaloid saturated water into the oven dish (the wider the better for evaporation) then into the oven. The solution should be no more than 3 cm deep (otherwise evaporation will take ages). Set the oven to fan and around 70 – 100 degrees Celsius (depending how much you trust the internal thermometer of the oven). Remember, if the mixture/solutions reach a temperature higher than 100 degrees Celsius then there is a high risk of alkaloid loss. Keep the oven door ajar to encourage evaporation. Check every 30 minutes (mine took around 4 hours, but I have an awful oven). Use a knife/scraper to scrape the resin onto the cooking parchment (baking paper will do) for each of storage. The resin is pretty oily and sticky-icky so the parchment paper stops it sticking to everything.
Voilà!
Consumption
The resin is great for storage and for reducing the physical volume of your dose.
Weighing the resin can tell you how strong your resin is: original kratom weight divided by resin/extract weight = the extract strength.
For example, from my latest batch using half measures of everything (see pics): 50g powdered kratom divided by 15g resin = 50/15 = 3.3. So, one gram of resin is the equivalent of 3.3 grams of dried powdered kratom! So we can say we have a 3x kratom resin extract.
Add the resin to a pot of hot water to create tea (you may want to mask the taste using honey, teas, vanilla, or within peanut butter, etc).
The resin can be put into gel caps and swallowed.
The resin can also be dried further and ground into an enhanced powder (however, sometimes the extracts are very oily and take a while to dry).
Kratom cannot be smoked, nor can the resin.
If properly prepared, the onset is ~50 – 120 minutes and lasts ~5 – 7 hours (gel caps take longer to dissolve).
Note: If more powdered kratom is used then the measurements should be increased accordingly, although this tek will be quite forgiving (to the same ratio, i.e., if 200g powdered kratom is used then 6 litres of water is needed).
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