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What is high pressure autoclave?
High-pressure autoclaves are designed for pressures far above 100 bar. The material properties must therefore be able to withstand such a load. All connections, i.e. valves, measuring devices and closures, are specially designed for applications under the influence of high pressure and temperature.
What is autoclave reactor?
The autoclave reactor is a small cylindrical reactor, built to withstand high pressures, used to evaluate the kinetics of high-temperature, high-pressure reactions and the production of small quantities of specialty chemicals.
How do I increase the pressure in my reactor?
An inert gas can be used along the feed streams to increase the pressure. Agitation another approach to increasing the frequency of collision of reactant molecules thus increasing pressure. Increasing the temperature of the reactor can also lead to an increase in pressure.
What is vertical autoclave?
Vertical autoclave, also known as steam sterilizers and top loading sterilizers, is a sterilizing machine that comes in a cylindrical shape. These machines help in sterilization of medical equipment, surgical instruments to name a few.
How do you use autoclave?
- Place the items to be sterilized in the autoclave. The door is locked.
- A vacuum pump sucks the air from the chamber.
- The temperature reaches the correct level.
- Steam kills bacteria and microbes.
- Steam is released, the door is opened and items are ready for use.
What reactor type is also called an autoclave reactor?
What reactor type is also called an autoclave reactor? Fixed bed reactor. This type of reactor contains a stationary catalyst bed, and product flows over the catalyst to form the desired product. boiling water reactors and pressurized water reactors.
How many types of autoclaves are there?
The two basic types of steam sterilizers (autoclaves) are the gravity displacement autoclave and the high-speed prevacuum sterilizer.
Why Teflon is used in autoclave?
It is resistant to corrosion, acidic solution, and stable at high temperature. Generally, there are two types of Teflon lined autoclave: the threaded type and the flange type.
Which reactor is not recommended for high pressure reaction?
So CSTR, Batch reactors are not suitable.
What are the different types of reactors?
The three classical generic chemical reactors are the batch reactor, the continuous stirred-tank reactor (CSTR), and the plug flow tubular reactor (PFR). Each of these reactor types has its own unique characteristics, advantages, and disadvantages.
Is reactor a pressure vessel?
Reactor Pressure Vessels (RPVs) are large cylindrical steel vessels containing a core, cooling water and generated steam, that requires high reliability to withstand high temperatures and high pressures, and neutron irradiation, which makes the RPV the most critical pressure boundary in the nuclear power plant.
What is the role of pressure in autoclaving?
Essentially an autoclave is a pressure cooker that uses steam under pressure as its sterilizing agent. The increase in pressure (above atmospheric pressure) enables steam to reach higher temperatures. The extra pressure brings the boiling temperature of water higher. In fact, around 20°C higher.
Why is pressure important in an autoclave?
The extra pressure in an autoclave means that water boils at a temperature higher than its normal boiling point—roughly 20°C hotter—so it holds and carries more heat and kills microbes more effectively.
How many types of autoclaves are there?
The two basic types of steam sterilizers (autoclaves) are the gravity displacement autoclave and the high-speed prevacuum sterilizer.
Can a pressure cooker be used as an autoclave?
A pressure cooker works just as well as autoclaving, especially for small batches. Just like an autoclave, the pressure cooker chamber reaches temperatures high enough to kill bacteria and mold spores.
Buchiglas – novoclave – high pressure reactor
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High Pressure Autoclaves – Vessels up to 5.000 litres | Made in Germany
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high pressure reactor
Laboratory high pressure / high temperature reactor (HPHT)
Standard Version:
Reactor volume: 100 – 600 ml
Pressure: -1 (FV) to +400 bar
Temperature: -20 °C to + 400°C
Material: stainless steel, (Hastelloy® +400°C)
High-Pressure Version:
Reactor volume: 100 – 600 ml
Pressure: -1 (FV) to +500 bar
Temperature: -20 °C to + 500°C
Material: stainless steel, (Hastelloy® +400°C)
This is our new high pressure and high temperature HPHT (high pressure high temperature) autoclave novoclave. This high pressure reactor system is designed for processes involving high pressures and temperatures. Safety features guarantee safe reactions under highest pressure. Designed, manufactured, and tested according to PED, AD2000. Electrical heating with built-in automated tap water cooling for fast and precise temperature control and programmable PID controller for operation at device or via PC.
The modular setup of the novoclave system allows for changing the vessel size from 100ml up to 600ml using the same cover plate and electric heating block. Vessels are available in the following volumes: 100 / 200 / 300 / 450 / 600ml. Despite changing vessel sizes, the optimal vessel geometry (i.e. relation between diameter and length) is maintained.
The stainless steel or Hastelloy® reactors ensure high corrosion resistance. The magnetic stirrer drive ensures efficient mixing and stirring of the process media as well as excellent heat transfer.
A wide range of accessories is available.
Talk to us to define the right setup for your specific need.
High Pressure Reactor Manufacturers
It is mounted on the vent line to maintain constant pressure inside the autoclave. The pressure can be set initially, either manually, pneumatically or electronically. Once the set pressure is exceeded, the excess pressure is released until the autoclave pressure becomes equal to or below the set pressure. The pressure release is slow and gradual and the set pressure can be varied at any point.
a) Manual Back Pressure Regulator : The pressure can be set initially on the gauge, by manually varying the knob until the gas comes out.
b) Electronically actuated digital pneumatic back pressure regulator : In this, the pressure is set digitally & can be released at a preset rate of pressure release. (6 bar air supply is required).
Stirred Autoclave High Pressure Reactor 500ml-5ltr
Heating Cooling Circulators ×
Open Bath Heating Circulator
It is used to heat jacketed autoclave from ambient to 150°C by circulating thermic fluid inside thejacket. It consist of bath, pump, level switch, heater & internal cooling coil for cooling from hightemperature to ambient temperature using chilled water or brine solution.It is suitable for reactors up to 5 liter volume.
Optional
Ex-proof heating bath
Closed Loop Heating Circulator (CLH)
It is used to heat jacketed autoclave from ambient to 350°C by circulating thermic fluid. Itconsist of a closed pressure withstanding tank, magnetically coupled pump, heater, levelindicator & internal cooling coil for cooling from high temperature to ambient temperatureusing chilled water or brine solution.
Suitable for reactors up to 100 ltr volume.
Optional
Ex-proof circulator
Low temperature open bath circulator (CB)
It is used to cool or control reactor temperature to -50°C by circulating thermic fluid cooled toup to -75°C inside the jacket or internal coil. It consists of a bath, pump, compressor, condenser& level switch.
Suitable for reactors up to 100 ltr volume
Heating Cooling open bath circulator (HCB)
It is used to heat, cool & control reactor temperature by circulating thermic fluid in theautoclave jacket. It consists of a bath, pump, heater, compressor, condenser & level switch.
Temperature range: -25°C to 175°C.
Suitable for reactors up to 5 ltr volume
Closed loop heating cooling circulator (CLS)
It is used to heat, cool & control reactor temperature by circulating thermic fluid in theautoclave jacket. It consists of a bath, pump, heater, compressor, condenser & level switch.
Temperature range: -35°C to 200°C / -80°C to 180°C.
Suitable for reactors up to 1000 ltr volume.
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